Status : Verified
Personal Name Rocha, Reina Danielle P.
Resource Title Optimization of drying parameters of eggshell calcium powder preparation
Date Issued 13 June 2016
Abstract A survey of studies on eggshell calcium powder production revealed that there is a wide variation in terms of methodology, specifically with respect to drying conditions such as time (60-1000°C) and temperature (10 to 120 min.). The aim in this study was to establish and optimize drying process factors (temperature and time) of eggshell calcium powder production using a two factorial response surface methodology design. Optimization criteria include the minimization of water activity (0.30 - 0.85) and maximization of calcium content (~ 40%). Two quadratic models, which predicted the effects of drying temperature (T, 60 - 150 °C) and time (t, 10 - 120 min.) on water activity and calcium content, were generated: aw = 1.044 - 2.36 x 10 exp -3 T - 1.285 x 10 exp -3 t - 1.235 x 10 exp -5 (Txt) %Ca= 31.68 + 3.8 x 10 exp -2 T + 5.89 x 10 exp -2 t - 3.25 x 10 exp -4 ( T x t ) Drying at 137 °C for 10 min. was predicted to meet optimization criteria and was selected as the optimal solution. Verification experiments, using optimal (137 °C, 10 min.) and non - optimal (60 °C, 10 min.) drying conditions, were used to validate the accuracy of the predictive models. The water activity of "optimal" (aw 0.518 ± 0.03) and "non" - optimal powders (aw 0.868 ± 0.01) were generally shown to be lower than their predicted responses (0.690 ± 0.03 and 0.882 ± 0.03 respectively). While their calcium contents (37.57 ± 1.17 % and 36.52 ± 1.26 %) were shown to be higher than predicted (37.025 ± 1.01 and 34.35 ± 1.01). In general, actual values were found to be better than their predicted values. Verification experiments confirmed that the generated models predicted responses within tolerance intervals and can produce fail safe results.
Degree Course Bachelor of Science in Food Technology
Language English
Keyword Eggshells--Drying--Philippines
Material Type Thesis/Dissertation
Preliminary Pages
878.88 Kb
Category : F - Regular work, i.e., it has no patentable invention or creation, the author does not wish for personal publication, there is no confidential information.
 
Access Permission : Open Access